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NEI Expands Selection of Materials for Lithium-ion & Sodium-ion Batteries

January 13, 2022

Somerset, New Jersey (USA) – Today, NEI Corporation announced customers can now order from an expanded selection of cathode, anode, and solid electrolyte materials for both lithium-ion and sodium-ion batteries. The company, which is a leader in the development, manufacture, and supply of specialty materials, has been a go-to organization for producing and delivering custom powders and dispersions of particles in liquids and polymers, as well as electrodes cast on metal foil.

NEI offers a variety of battery materials, with a particular forte in producing specialty materials with compositions and particle morphologies that are not commonplace. In addition, NEI has expertise in producing composite particles that have a surface coating. Off-the-shelf products are sold under the tradename NANOMYTE®.

“We want our customers to easily access high quality and consistent battery materials so they can focus on their core mission,” said Dr. Ganesh Skandan, CEO of NEI Corporation. “The NEI team stands ready, willing, and able to produce and supply materials that our customers want, in any quantity needed, for them to pursue their commercialization efforts.”

Particle Size Distribution graph of Na0.44MnO2+x , which is typical of most of NEI's sodium based cathode/anode powders

Particle size distribution (PSD) of Na0.44MnO2+x , which is typical of most of NEI’s sodium based cathode/anode powders.

NEI has been routinely supplying increasing quantities of simple metal oxide compositions such as Na0.44MnO2+x and Na0.7MnO2+x with a narrow particle size distribution. The portfolio of sodium-ion compositions now includes more complex materials, such as sodium iron phosphate (NaFePO4), sodium nickel phosphate (NaNiPO4), sodium titanium phosphate (NaTi2(PO4)3), sodium chromium oxide (NaCrO2), and others. The average aggregate particle size (D50) for most compositions can be tailored to be in the range of 1 – 2 µm, with the primary particles being much smaller. The particle structure can be further tuned to include a surface coating of carbon or a conducting polymer, such as polyaniline, PANI, or an ionically conducting ceramic material. Some of the materials have been tested and validated in-house using half-cell configuration (i.e., sodium metal anode). For example, Na0.44MnO2+x has a second cycle charge and discharge capacity that is > 105 mAh/g.

Second cycle charge/discharge profile of Na0.44MnO2+x cathode powder

In addition to engineering the particle morphology, all sodium-based cathode and anode materials can be supplied as cast electrodes on a current collector of choice. Customers can specify the active material, binder content, amount of conducting carbon and active material per unit area (in case of cathode and anode).

NEI Corporation has built a reputation for supplying consistent and high-quality solid electrolyte materials – oxide materials, such as Al-doped lithium lanthanum zirconium oxide (LLZO) and tantalum-doped LLZO (LLZTO), phosphate compounds, such as LATP or LAGP, and a variety of sulfide-based materials. While the average particle size (D50) for these standard powders is in the 3 – 5 microns range, customers can request a smaller D50.

Cole-Cole plot of sintered LAGP pellet

Cole-Cole plot of sintered LAGP pellet

The ionic conductivity of the oxide materials, measured in-house using Electrochemical Impedance Spectroscopy in a test cell shown in the inset of the picture (left), is in the range of 1 x 10-4 S/cm to 5 x 10-4 S/cm, and that of sulfides can be as high as 1 x 10-3 S/cm.

A recent and exciting development has been the offering of composite solid electrolyte materials in the form of either a polymer-based dispersion or cast membrane. Customers can choose any oxide ceramic solid electrolyte and a base polymer or co-polymer from PEO, PVDF, PVDF-HFP, and PAN. The type of lithium salt in the polymer can be selected from LiTFSI, LiClO4, LiFSI, and LiBOB.

In addition to increasing the suite of materials being offered, NEI has developed new materials synthesis capabilities, which serve as demonstration stations for exploring new compositions that are difficult to produce using conventional processing. A case in point is precursor materials obtained from recovered nickel, cobalt and manganese salts from recycled lithium-ion batteries. The solution-precipitation setup, installed at NEI, serves as a test-bed to determine processing parameters for materials such as NMC532 and NMC622, or any mixed metal oxide for that matter.

There is also increasing interest in cathode materials that are fluorinated and/or contain vanadium, which as multiple valence states and can lead to high capacities. To this end, NEI has produced LiFeSO4F and LiVPO4F with a high degree of crystallinity and phase purity.

Overall, the introduction of these new materials and processes will provide new capabilities to lithium battery developers and manufacturers to enable practical solid-state batteries. Dr. Skandan adds, “It is exciting for the team at NEI to tread on uncharted waters and explore synthesis and processing of new materials, and particularly using newly developed processes. We welcome the opportunity to serve the needs of the Battery community.”

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About NEI: Founded in 1997, NEI develops, manufactures, and sells advanced materials for a broad range of industrial customers around the world. The company’s core competencies are in designing, developing, and producing products that meet the specific application needs of its customers. More importantly, NEI is a solutions provider, working closely with customers to produce and implement materials for their applications. NEI’s products, which are sold under the registered trademark NANOMYTE®, are backed by a suite of issued and pending patents. NEI’s products include:  Lithium-ion Battery Materials, Na-ion Battery Materials, Functional & Protective Coatings, and Specialty Nanoparticle-based products. NEI also offers associated materials characterization and testing services.

For more information, give us a call or email us.

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NEI Coating Product Update

NANOMYTE® TC-4001-UVP Offers Protection Against Damage by UV-C Radiation Used to Disinfect Coronavirus

May 6, 2020

Somerset, NJ (USA) – NEI Corporation announced today that its newly developed NANOMYTE® TC-4001-UVP product has been shown to offer protection against damage from short-wavelength ultraviolet radiation. Ultraviolet radiation in the 100nm – 280nm wavelength range, also referred to as UV-C, is increasingly being considered as a means for disinfecting surfaces that large numbers of people are likely to come in contact with, such as parts of transit systems, theme parks, cinema theaters, public restrooms, airports, and other areas of high traffic. The COVID-19 virus has made frequent cleaning of surfaces a top priority for maintenance managers of high traffic areas. However, UV radiation causes significant damage to painted surfaces by creating free radicals that then cause polymer degradation. The NANOMYTE® coating offers protection for surfaces exposed to UV-C radiation.

TC-4001-UVP Spectroscopic Graph

NANOMYTE® TC-4001-UVP Spectroscopic Measurements

NANOMYTE® TC-4001-UVP shows remarkable ability to block UV-C, as evidenced by spectroscopic measurements shown in the adjacent figure. All radiation below 350nm is blocked completely by a film that is only 1/5 mil (5 microns) thick. The transparent coating is a single component formulation designed to protect metals and other surfaces from degrading, preserving their structural integrity and appearance. The hard, dense, and smooth coating is a composite consisting of organic and inorganic phases. It resists scratching and chipping and adheres strongly to bare, pretreated, or painted metal surfaces. A variety of other surfaces may be coated as well, such as plastics and composites. The coating is easily applied by immersion, spraying or brushing, in thicknesses ranging from microns to mils, and is available in glossy or matte finishes.

NEI’s extensive line of functional coatings, which includes NANOMYTE® TC-4001-UVP, is already in commercial use in many industrial, aerospace, consumer goods, wireless communication, and other sectors.

1000 Hours Constant UV Exposure: Polycarbonate in QUV Chamber with UVA 340 Lamps @ 0.9 W/m2

The company’s approach has been to be open and receptive to new applications brought to it by its customers. A typical interaction begins by applying the coating on the customer’s parts for evaluation. Parts are either coated at NEI’s applications laboratory or the customer procures a sample quantity of liquid coating for in-house application. The implementation process then moves through pilot scale tests and eventual qualification. NEI’s engineers support the development and qualification efforts of its customers every step of the way, including drawing up technical specifications and engaging with third party coating applicators, if necessary.

Additional Information: NANOMYTE® TC-4001-UVP Technical Data Sheet (TDS) | Safety Data Sheet (SDS)

View / Download Press Release (pdf) ↓

About NEI Corporation:

NEI is an application-driven company that utilizes materials science & chemistry to develop and produce Advanced Materials. NEI offers an array of Functional Coatings for metal and polymer surfaces. The coatings have tailored functionalities, such as Easy-to-Clean, Anti-Ice, Self-Healing, Corrosion resistant, Anti-Fog, and Abrasion Resistant.

For more information, give us a call or email us.

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New Anti-ice System Advances to Next Technology Level

Full-scale Prototype Demonstration of a New Hybrid Technology to Prevent Icing on Aircraft and Drones

January 15, 2020

Somerset, NJ (USA) – Invercon Inc. and NEI Corporation announced today that their newly developed de-icing system was tested successfully at the NASA Glenn Research Center’s Icing Research Tunnel. The test was witnessed by engineers and scientists at the Research Center, as well as from the industry. The Invercon-NEI team met the objective of demonstrating a low power anti-ice system in conjunction with NEI’s NANOMYTE® SuperAi anti-ice coating that prevents ice accretion on the leading edge of an airfoil. The test was performed on a full-size airfoil under simulated in-flight conditions, following nearly two years of development and laboratory testing.

All commercial aircraft have a built-in ice protection system, which could be either a thermal, thermo-mechanical, electro-mechanical, or pneumatic system. A common issue with de-icing devices is that they consume substantial power. Aircraft generally look to reduce power consumption, and with the advent of battery-powered aircraft, mechanisms or features that reduce power consumption are critically important. Icing presents a particular challenge for commercial and military drones, where ice can build up on the wings and propellers and result in crashes. In fact, the current practice is not to fly drones when icing conditions are predicted. Applying a passive anti-ice coating that functions synergistically with an active de-icing device is an attractive hybrid approach, which the team of NEI and Invercon has now demonstrated on full-scale prototypes.

NEI’s NANOMYTE® SuperAi anti-ice coating is a durable coating, suitable for permanent application. The coating leads to a lubricating surface that drastically reduces the adhesion strength of ice – by as much as 80%, compared to bare polished aluminum. The coating is usually applied by spraying, similar to conventional painting. NANOMYTE® SuperAi coating is available for commercial use.

Figure 1: MQ-1 wing test section installed in the IRT tunnel.

Invercon has developed a new, retrofittable, electro-pneumatic deicing system that combines the most attractive aspects of several existing systems without their associated drawbacks. The Invercon system requires remarkably low power (≤ 2.5 kW), is retrofittable on any airfoil, adds very little weight (~50 lbs), and is durable enough to last the life of the aircraft once retrofitted. Importantly, the system looks, feels, and acts like the original leading edge and can provide millions of maintenance-free deicing cycles. The entire wing test section (Figure 1) was coated with NANOMYTE® SuperAi.

Invercon successfully completed icing tests of the electro-pneumatic deicing system at NASA Glenn’s Icing Research Tunnel (IRT) under a full range of representative icing conditions. The Invercon system was able to provide continuous deicing of the wing section leading edge over all of the test conditions ranging from temperatures of -3°C to -20°C with various liquid water content. Typically, the system allows ice to accrete for about 2 minutes and then completely sheds upper and lower surface ice upon system activation.

The testing at NASA’s IRT, which is the longest running icing facility in the world, has moved the hybrid technology to a readiness level of 6 (i.e., TRL6), which is a scale used by NASA and Department of Defense to gauge the maturity level of a technology.

Both NEI Corporation and INVERCON LLC are grateful for the financial support extended by the Small Business Innovation Research Program from the Air Force and NASA. The SBIR program funds product development efforts that reduce concepts to practice and then to prototypes, thereby reducing technology risk. The successful full-scale demonstration by the team has advanced a new technology to a state of commercial readiness.

View / Download Press Release (pdf) ⇓

About NEI Corporation:

NEI Corporation is an application-driven company that utilizes nanotechnology to develop and produce advanced materials. The company’s core competencies are in synthesizing nanoscale materials and prototyping products that incorporate the advanced materials. NEI offers an array of Advanced Protective Coatings for metal and polymer surfaces. The coatings have tailored functionalities, such as anti-corrosion, self-healing, scratch resistance, ice-phobic, and self-cleaning.

For more information, give us a call or email us.

About Invercon LLC:

Invercon’s mission is to develop advanced technologies that enable revolutionary leaps forward in aircraft performance and safety.  For rotorcraft, these include centrifugally powered, pneumatic actuation systems that can actively trim rotors and de-ice rotor blades using almost no power or weight, resulting in significantly improved performance and safety.  For fixed wing aircraft, Invercon has developed extremely low power deicing solutions using a novel electro-pneumatic actuation approach.

For more information, give us a call or email us.

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NEI Addresses Unmet Self-Healing Needs for Transparent Polymeric Films Market

June 18, 2019

Somerset, NJ (USA) – NEI Corporation announced today that it has successfully demonstrated application of its NANOMYTE® MEND 1000 self-healing coating technology on PET film. The coated film is able to recover from repeated scuffing and scratching after heating to 60°C, typically using hot water or a hair dryer. Self-healing is achieved by a thermally-induced, physical self-healing phenomenon which leads to gap closing and crack sealing. This allows the coating to heal repeatedly at the same defect location, which helps to reduce life cycle costs by increasing the service life of the coated material. NEI’s MEND coatings exploit a unique phase-separated morphology that facilitates delivery of the self-healing agent to the damage site (such as a scratch or crack), thereby restoring the coating appearance & function.

There are numerous applications for polymeric films produced in the roll-to-roll coating industry, including signage, vehicle wraps, interior and exterior wall wraps, and protective overlaminates such as those commonly found on touchscreens or installed over window glass. These films are typically relied upon to protect from physical damage or to reduce the transmission of light while providing heat rejection, features which are in high demand for automotive and architectural glass.

Roll-to-roll processes present unique challenges for coatings in terms of the speed and temperature necessary to achieve a sufficient cure. Line speed requirements will often dictate that curing occur within a period of 1-2 minutes at temperatures around 100°C. To increase the speed of cure to better suit continuous, roll-to-roll processing of coated film, NEI now supplies a catalyst additive which can reduce the dry-to-touch (DTT) time to as little as 1 minute at 100°C (exact time and temperature will depend on wet film thickness and other processing conditions), which has allowed its customers in the roll-to-roll coating industry to successfully process the coating.

NEI supplies three versions of its popular NANOMYTE® MEND self-healing coating products to meet different performance and processing requirements:

  • MEND 1000 – heat cure, 60°C healing temperature
  • MEND 2000 – heat cure, 25°C healing temperature
  • MEND 3000 – ambient cure, 60°C healing temperature

The coatings are supplied as 2 components, Parts A and B, which are mixed before application. Further customization can then be accomplished with the addition of a catalyst to speed up curing and/or a reducer to adjust viscosity. NEI can also supply coating formulations with increased viscosity to meet process requirements. Please refer to the product technical datasheets for further guidance. To enhance light-stability and weatherability, NEI also offers its MEND product line with UVP technology to protect sensitive surfaces by blocking UV light while preserving the coating performance. This feature can be critical for some applications, such as those which may cause yellowing of sensitive polymers. NANOMYTE® UVP coating products have demonstrated their ability to endure a minimum of 1000 hours of weatherability testing per ASTM D4587, “Accelerated Weathering under Fluorescent UV-Condensation Exposure”. The testing was performed in a QUV chamber under the conditions specified in ASTM G154, Cycle 1, the most commonly used exposure cycle designed to simulate severe outdoor service conditions.

NANOMYTE® MEND coating products can be applied by a variety of processes, including spraying, dipping and flowing. NEI also offers in-house coating services for customer’s parts as well as coating development services, wherein coating formulations are created to address specific customer requirements.

Links to Technical Data Sheets:

Additional Information: Safety Data Sheets ♦ MEND Product Page ♦ Demonstration Video

View / Download Press Release (pdf) ↓

About NEI Corporation: NEI Corporation is an application-driven company that utilizes nanotechnology to develop and produce advanced materials. The company’s core competencies are in synthesizing nanoscale materials and prototyping products that incorporate the advanced materials. NEI offers an array of Advanced Protective Coatings for metal and polymer surfaces. The coatings have tailored functionalities, such as anti-corrosion, self-healing, scratch resistance, ice-phobic, and self-cleaning.

For more information, give us a call or email us.

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The Development of NEI’s Anti-Ice Coating Technology for the Aerospace Industry

A Case Study of NANOMYTE® SuperAi from Concept to Implementation

The leading edge of the wing is where icing occurs

A manufacturer of de-icing systems brought up the idea of combining an active de-icing system with a coating that easily sheds ice. Ice formation on the leading edge of an aircraft is a common aviation danger, playing a key role in several catastrophic accidents over the years that have killed people and destroyed aircrafts. All commercial aircraft have a built-in ice protection system, which could be either a thermal, thermal-mechanical, electro-mechanical, or pneumatic system. A common issue with de-icing devices is that they consume substantial power.  Aircraft generally look to reduce power consumption, and with the advent of battery-powered aircraft, mechanisms or features that reduce power consumption are critically important. The aspect of reduced power is also relevant for battery powered drones. Applying a passive anti-ice coating that functions synergistically with the active de-icing device is an attractive approach. The advantages are reduced power consumption, improved service life of mechanical components, lighter electronics and extra protection in case of failure of active device.

The challenge presented to the engineers and scientists at NEI Corporation was to develop and demonstrate a coating that exhibits durable anti-ice performance and satisfactory wear and erosion resistance. More importantly, it needed to be practical for retrofitting in-service aircraft as well as be used by OEMs. In order to address the need, NEI developed its NANOMYTE® SuperAiTM coating technology to have the following features:

  • Extremely lubricating surface
  • Superior ice adhesion reduction factor
  • Thin coating (< 1 mil or 25 microns), providing a light weight solution
  • Durable anti-ice performance, suitable for permanent application
  • Room temperature cure
  • Easy application by spraying, dipping, or brushing

The development of the SuperAiTM coating started after numerous discussions with engineers at a major low-power ice protection system manufacturer. They brought to our attention the two basic technical requirements for an anti-ice coating to be applied on their de-icing systems, i.e., lower ice adhesion and durable anti-ice performance. We demonstrated both attributes after extensive experiments in NEI’s laboratory and iterative testing at an icing wind tunnel facility with prototype de-icing devices. The ice adhesion measurements taken at NEI were corroborated by work done at the Penn State Adverse Environment Rotor Test Stand (AERTS) facility, which repeatedly showed an ice adhesion strength as low as ~1.8 psi for the SuperAiTM coated aluminum substrate – this represents an 80% reduction compared to an uncoated polished aluminum substrate (Figure 1). Figure 1 shows a pure adhesive failure when an ice column was pulled off the SuperAiTM coated substrate. In contrast, a cohesive failure of ice is seen for the uncoated aluminum substrate.

Figure 1: Ice adhesion strength and locus of failure of SuperAiTM coated aluminum as compared to those of uncoated polished aluminum

To demonstrate the enhanced de-icing efficiency of a de-icing device with the use of SuperAiTM, coated prototypes of electro-mechanical and thermal-mechanical expulsion de-icing systems were tested in an icing tunnel under simulated in-flight icing conditions at our collaborator’s facility. Figure 2 shows the SuperAiTM coated leading edge being assembled with the thermal-mechanical expulsion de-icing system. We have repeatedly demonstrated that improved de-icing efficiency, along with a 45-70% reduction in power consumption of the active de-icing systems could be achieved with the use of the newly developed anti-ice coating (Figure 3).

Figure 2: Installation of leading edge and thermal-mechanical expulsion de-icing system assembly.

Figure 3: Snapshots taken from recording of icing tunnel test showing complete de-icing on coated leading edge (bottom) and no de-icing on uncoated leading edge (top), at power consumption level 70% lower than that of the nominal power needed for a regular functional uncoated de-icing system.

Abrasion resistance is of great importance for the targeted application. Figure 4 shows that the SuperAi coating was barely scratched at the wear track after 200 cycles of Taber abrasion. Note that the CS-10F Calibrase® wheel used in the test is composed of a binder and abrasive particles such as aluminum oxide and silicon carbide. The testing conditions simulate normal service abrasion and wear. Further, the contact angle at the wear track was measured to be 103° (vs. 105° of fresh unabraded surface), indicating that the hydrophobicity of the surface was minimally affected by the abrasion. The ice adhesion measurement at the wear track showed that the coating remained highly icephobic after 200 cycles of Taber abrasion (Figure 5).

Figure 4:  Optical micrograph taken at the wear track after Taber test showing excellent abrasion resistance of the SuperAiTM coating.

Other important aspects of an anti-ice coating for aircraft include its ability to resist rain erosion, chemical and solvent resistance, resistance to icing-deicing cycles and weatherability. These aspects were investigated with various durability tests. As can be seen in Figure 5, the SuperAiTM coating could survive repeated icing-deicing cycles. There was little change in ice adhesion after immersion in jet fuel, Skydrol® (an aviation hydraulic fluid), and water for an extended period of time. Further, the ice adhesion strength was minimally affected by abrasion, high-pressure power wash and UV-Con exposure.

Figure 5:  Ice adhesion results for SuperAiTM after various durability tests.

In summary, we were able to address an important need in the industry, using a disciplined and focused product development effort. The case study presented here is representative of the application-driven coatings development effort we undertake to address a problem or an opportunity. We work directly with customers and seek to develop, demonstrate, and implement a solution.

For more information, give us a call or email us.

NEI Corporation is extremely mindful of maintaining the confidentiality of its customer’s information, even without a non-disclosure agreement. Specific and sensitive information relating to customers have been withheld.

Download Case Study (pdf) ↓

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NEI Patented Coatings Technology Brief

NEI Corporation’s Patented Technologies Provide a New Perspective on Coatings and Surface Treatment

Gains in productivity and efficiency are possible when a coating or surface treatment provides functionalities beyond the usual protective and aesthetic properties. This realization has sparked great interest in functional coatings in recent years for applications that traditionally have not used paints or coatings. A good example is the use of anti-ice coatings on power transmission lines. Mitigating ice accumulation will help prevent power outages, which has a tangible and beneficial economic impact. Another example is the use of a surface treatment to increase the efficiency of power generation turbines.

Examples of functionalities of interest for both industrial and consumer applications include:

  • Self-Healing: the coating or surface treatment autonomously repairs damage
  • Hydrophobicity: coated surfaces vigorously repel water droplets
  • Oleophobicity: prevents “oil” molecules from sticking to the surface
  • Self-Cleaning / Easy-To-Clean: minimizes or eliminates the need for chemicals during washing
  • Adhesion Enhancement: promotes ultra-strong bond between the coating and the surface

While great strides have been made in academic circles to understand the different surface phenomena of these so called ‘smart coatings’, commercial products to date have met with limited success because they are not engineered to meet all of the functional performance requirements that an application may need. For example, commercially available superhydrophobic coatings repel water droplets, but do not prevent the diffusion of water vapor – minimizing moisture ingress is a critical functionality for most protective coatings.

More often than not, many of the functionalities mentioned above need to be integrated into a single coating or surface treatment. For example, a transparent coating that resists finger printing also needs to be scratch resistant and durable. A coating that prevents fogging in eyewear and other transparent surfaces must also be durable and resistant to chemicals. Further, in order to meet the cost criteria, application of the coating must be compatible with conventional coating methods such as spray, dip, brush or flow. Over the past few years, NEI Corporation’s concerted efforts to develop and implement practical, multi-functional coatings are now coming to fruition.

Backed by a bevy of issued and pending patents, NEI has introduced an array of coating products under the registered trade name NANOMYTE®. For example, NANOMYTE® MEND is based on US Patent 8,987,352, where a thermally induced, physical self-healing phenomenon leads to gap closing and crack sealing. The self-healing coating involves a unique phase-separated morphology that facilitates the delivery of the self-healing agent to the damage site (such as a scratch or crack) thereby restoring the coating appearance & function. Utilizing commonly available polymer materials and nanoparticles arranged in a unique morphology to achieve self-healing, MEND offers a practical self-healing solution to common polymer coating systems. In response to the need for waterborne, self-healing coatings for non-metallic substrates, NEI developed a waterborne, polyurethane-based, self-healing coating. NANOMYTE® MEND for wood (US Patent 8,664,298) specifically targets the wood cabinet market. A more recent patent-pending version of MEND, referred to as MEND-RT, allows self-healing at near ambient temperature. It is used as the inter-layer of a coating stack and has been shown to enhance the corrosion resistance of traditional coating systems. The MEND coating platform is based on polyurethane, but the principle can be applied to other coating systems as well.

Self-healing principles can also be applied to surface treatments of metals, whereby the pretreatments can mimic the performance of chromate conversion coatings. To this end, NEI has developed a series of pretreatments for different metals where a chemical self-healing mechanism imparts corrosion resistance. For example, NANOMYTE® PT-60 is a patent-pending conversion coating for use on magnesium alloys. The nanoscale structure of the surface allows ions to diffuse to the damage site, forming a barrier that prevents further corrosion. In addition, PT-60 has been engineered to act as a tie layer that bonds the overlying primer with the metal, thereby leading to excellent performance in the field. Similarly, NEI’s NANOMYTE® PT-10M provides self-healing protection for aluminum, while patent-pending PT-20 is designed for use on steel, and PT-30 (US Patent 8,741,074) is used on copper alloys.

As previously mentioned, combining multiple functionalities in a coating, such as self-healing and superhydrophobicity, presents new opportunities not available until now. For example, NEI has been issued a patent (US Patent 8,968,459) for a superhydrophobic coating composition that also has a self-healing function similar to that of plant leaves. This self-healing, superhydrophobic coating mimics lotus leaves, which maintain their superhydrophobicity by repairing the damaged surface layer with a continuously-secreting hydrophobic epicuticular wax. Equipped with the ability to repair or renew itself, the novel NEI coating overcomes the durability problem of traditional superhydrophobic coatings.

Durable hydrophobic coatings are highly desirable for numerous applications as they usually impart easy-to-clean and stain-resisting properties to surfaces. For aesthetic reasons, there is also a need for a thin, transparent, easy-to-clean coating that does not add excess weight and does not change the appearance of the substrate to be coated. Further desirable properties of such coatings include a high degree of scratch/abrasion resistance, excellent adhesion, and chemical resistance, all of which are critical in maintaining a durable coating. In addressing these needs, NEI’s recently developed NANOMYTE® SuperCN and SR-100EC products are patent-pending transparent coatings with a unique combination of properties, including easy-to-clean and stain-resisting properties, excellent abrasion/scratch resistance, as well as good adhesion with a variety of substrates – including polymers, metals, and ceramics.

Scratch resistance is a sought-after property for coatings in a variety of applications, such as ophthalmic and sports-wear lenses, automobile and airplane windows. Plastic substrates, such as polycarbonate and acrylic, can scratch easily and lose transparency quickly during daily use and maintenance. Hard and optically transparent coatings for plastic substrates possess a significant market potential. NEI offers a patented (US Patent 9,006,370) transparent, scratch-resistant coating called NANOMYTE® SR-100, which exhibits significantly better abrasion resistance than commercially available, scratch-resistant coating products. A matte version of SR-100 has also been developed and is now commercially available.

Adhesion enhancement is usually achieved by using adhesion promoters and surface treatment techniques. A recently allowed NEI patent application on adhesion promoter describes a surface pretreatment composition that is chromate‐free. The environmentally-friendly, waterborne pretreatment promotes adhesion between the metal substrate and overlying paint layer by acting as a “double‐sided bonding agent,” while at the same time improving corrosion resistance. The novel composition comprises organo-functional silanes but functions differently from traditional silane treatment. The composition results in a thin film coating having a graded structure, i.e., an inorganic oxide layer that bonds strongly with steel and a loosely crosslinked top layer containing functional groups that can further crosslink with paint overlay. The new technology has value to applicators who paint metal structures, such as bridges, ships, and other steel structures. It is also applicable to industrial painting operations such as coil and spray coatings. The patented chromate‐free pretreatment for steel, offered commercially as NANOMYTE® PT-20, represents a significant advancement in the state‐of‐the‐art for corrosion resistant technologies.

About NEI Corporation:
NEI is an application driven company that manufactures and sells Advanced Materials products, provides materials development services, and performs contract-based R&D for public and private entities. NEI’s products, which are sold under the registered trademark NANOMYTE®, are backed by a suite of issued and pending patents. NEI has built a strong manufacturing and R&D infrastructure that enables rapid transition of concepts to products. The company has a 10,000 square foot, state-of-the-art materials manufacturing and testing facility in Somerset, New Jersey, which includes high temperature furnaces with controlled atmospheres, mixing, blending and drying equipment, coaters, particle characterization instruments, corrosion testing equipment, polymer films & coatings characterization, and a Li-ion battery testing laboratory. Since its inception, NEI has partnered with small companies, large multinational corporations, U.S. Defense Laboratories, U.S. National Laboratories, and Universities. The relationships take on different forms, ranging from a strategic partnership to joint development efforts targeted at specific applications.

For more information, contact us at : +1 (732) 868‐3141 or sales@neicorporation.com

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Latest Test Results Confirm Performance of NEI’s Newly Optimized Anti-Ice Coating

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October 25, 2016

Somerset, New Jersey (USA) – NEI Corporation announced today that it has enhanced the performance of its anti-ice coating, NANOMYTE® SuperAi, and confirmed its efficacy through rigorous testing under a variety of icing conditions. SuperAi is a nanocomposite coating that imparts anti-ice properties to the underlying substrate. As a consequence of the engineered properties of the anti-ice coating’s formulation, it reduces ice buildup on surfaces, and provides a hard, dense, smooth finish.

Surfaces treated with NANOMYTE® SuperAi exhibit reduced ice adhesion, thereby reducing ice buildup. Precisely calibrated Ice Adhesion measurements showed that SuperAi has an Ice Adhesion Reduction Factor of greater than 5 (relative to a polished metal surface), indicating that NANOMYTE® SuperAi reduces the adhesion of ice by more than 80%, compared to smooth, bare metal and painted surfaces. The performance remains unaltered after repeated icing-deicing cycles, as well as after mechanical abrasion. Further, Icing Wind Tunnel experiments showed that SuperAi allows ice to be removed with minimal force, confirming its usefulness under practical use conditions.

superai_applications

NANOMYTE® SuperAi can be applied to a variety of substrates, including plastic, metal, glass, and ceramic. In some instances, a suitable primer may be required for long term durability of the anti-ice coating. SuperAi is a single component coating that is easily applied by spray or brush. The dry film thickness can be adjusted to be in the range of 5 – 25 microns (1/5th to 1 mil), and only one coat is required to cover the substrate. Current applications include occurrences where ice removal is a challenge (e.g., wind turbine blades, power transmission lines and cables, cellular phone towers, windshields and other glass surfaces in automobiles, aircraft wings, and unmanned aerial vehicles, UAVs). SuperAi also provides corrosion protection, which is an added benefit. The use of SuperAi enhances productivity for the user and provides rapid payback, as well as a good return on investment.

Contact us to obtain detailed test results on NANOMYTE® SuperAi.

Additional Information: NANOMYTE® SuperAi Technical Data Sheet | Safety Data Sheet

For more information, contact:
Ms. Krista Martin
+1 (732) 868‐3141
sales@neicorporation.com
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View / Download Press Release (pdf)

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NEI Releases a Newly Improved Version of NANOMYTE® SuperCN – a Durable, Hydrophobic / Oleophobic Coating

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February 29, 2016

Somerset, New Jersey (USA) – NEI Corporation announced today that it has introduced an improved version of its NANOMYTE® SuperCN coating. NANOMYTE® SuperCN – a micron-thick, transparent, and highly durable hydrophobic / oleophobic coating – was originally developed for promoting dropwise condensation in condensers to enhance heat transfer efficiency. The newly updated version has increased SuperCN’s ability to repel water and oils, with an improved adhesion to substrates, higher abrasion resistance, and better chemical and solvent resistance, all while remaining highly transparent. The SuperCN coating exhibits excellent anti-fingerprinting, anti-fouling, stain-resistant and easy-to-clean properties. The coating does not change the appearance of the substrate to be coated.

NEI’s SuperCN coating is based on a patent-pending composition comprised of sustainable functionalized perfluoropolyethers (PFPEs) that do not contain perfluorooctanoic acid (PFOA). Although PFPEs are known for their non-stick and lubricating properties, it has been a major technical challenge to incorporate them into a stable formulation that can lead to a coating with sufficient adhesion to various substrates. NEI’s SuperCN formulation overcomes this stability issue. Additionally, while PFPE-based, easy-to-clean coatings that are currently on the market generally form very thin (< 100nm) coatings, SuperCN coatings have a thickness of 2-5 microns, thereby creating a more mechanically stable coating that cannot be easily removed by abrasion or harsh cleaners and chemicals.

The contact angles of SuperCN-coated surfaces are 108 – 120° for water and 60 – 70° for hexadecane. The hydrophobicity and oleophobicity are maintained after thousands of rubs against a wool felt abrasion wheel (ASTM D1044). Additionally, the measured Δ Haze is less than 3% on polycarbonate substrates (CS-10F wheels, 500 gram load, 500 cycles). NANOMYTE® SuperCN adheres exceptionally well via covalent bonding with glass, ceramics, and basic metals (such as aluminum, zinc, and tin plate) with a standard industrial cleaning method. For passivated or noble metals – such as stainless steel, chrome, titanium, and copper alloys – NEI has developed a novel and specific surface pretreatment procedure to activate the surface before the application of SuperCN, leading to durable adhesion. Furthermore, the coating can also be applied to plastics (such as polycarbonate, PMMA, PET, polyurethane, and epoxy) with or without the use of a primer depending on the activation state of the substrate. NEI supplies a primer product, NANOMYTE® SR-Primer, which works well with a range of plastics.

The development of SuperCN was spurred by a high number of requests from customers that expressed a need for a relatively thin coating that is highly hydrophobic and oleophobic, but also hard and transparent. SuperCN is easy to use and ideally suited for a variety of commonly used consumer products, such as kitchen appliances, shower heads, hand rails, faucets, dining tables, shower doors, medical devices, optical lenses, and touch screens. The liquid coating solution can be applied by dipping, spraying, roll or flow coating, and is thermally cured at 80 – 150°C (a room temperature cure version is also available). NEI offers NANOMYTE® SuperCN in liter or gallon quantities, or through its in-house coatings service for customer parts. Finally, NEI also provides development services, wherein coating formulations are created to address specific customer requirements.

Additional Information:

About NEI Corporation:

NEI Corporation is an applications-driven company that utilizes nanotechnology to develop and manufacture Advanced Materials for a broad range of markets. The company’s materials and process technologies are protected by a total of seventeen patents. NEI offers an array of Advanced Protective Coatings for glass, metal and polymer surfaces. The coatings have tailored functionalities such as anti-corrosion, self-healing, scratch resistance, ice-phobic, and self-cleaning.

For more information, contact:

Ms. Krista Martin
+1 (732) 868‐3141
sales@neicorporation.com
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View / Download Press Release (pdf)

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DOE SBIR/STTR Programs Highlights NANOMYTE® SSE-10 Solid Electrolyte

A Safer Replacement for Highly Flammable Liquids Currently Used in Li-ion Batteries

NEI replaced liquid with solid material that allows for a no-liquid battery.

“An all-solid lithium-ion battery architecture, based on the solid electrolyte developed at NEI, will lead to safer, high-energy batteries that are needed for consumer and industrial applications. These applications include hybrid electric vehicles and electric vehicles, portable consumer customer electronics (laptops, tablets, digital cameras, smart phones, etc.), renewable energy technologies (solar and wind energy) that use electrochemical storage, and power tools.”

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Read the full article on the DOE website: http://science.energy.gov/sbir/highlights/2015/sbir-2015-11-b/

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